Calibration of a humidity chamber involves verifying and adjusting its performance to ensure it produces accurate and consistent humidity levels. Here's a step-by-step guide:
1. Preparation
- Read the Manual: Familiarize yourself with the chamber's operation and calibration instructions provided by the manufacturer.
- Gather Required Tools:
- Hygrometer or reference instrument (calibrated and traceable to national standards).
- Data logger (optional for continuous monitoring).
- Calibration salts or a humidity generator (if required).
- Tools for making adjustments, as per the chamber's specifications.
- Stabilize the Environment: Ensure the chamber is in a stable ambient environment free from significant temperature or humidity fluctuations.
2. Perform Calibration
Option A: Using Reference Instrument
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Place the Reference Instrument:
- Position the calibrated hygrometer inside the chamber at the test point.
- If the chamber is large, place sensors in multiple locations to ensure uniformity.
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Set the Humidity:
- Program the chamber to specific humidity levels (e.g., 30%, 50%, 70%, and 90% relative humidity).
- Let the chamber stabilize at each set point.
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Record the Readings:
- Compare the chamber's displayed humidity with the reference instrument's reading.
- Note deviations at each set point.
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Repeat for Temperature Variation:
- If the chamber has temperature control, perform the same tests at different temperatures to verify combined accuracy.
Option B: Using Saturated Salt Solutions
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Prepare Salt Solutions:
- Use salts like sodium chloride (NaCl) or magnesium chloride (MgCl₂) to create known humidity levels in sealed containers.
- Refer to a salt reference table for expected RH levels at specific temperatures.
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Place Solutions Inside:
- Place the solution container in the chamber and allow stabilization.
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Measure Humidity:
- Compare the chamber's readings with the expected humidity from the salt solution.
3. Adjust the Chamber (if needed)
- Use the calibration interface or manual adjustments to correct deviations.
- Follow the manufacturer’s procedure for entering calibration offsets.
4. Verification
- After adjustment, recheck all set points to confirm the accuracy.
- Perform a stability test by running the chamber for extended periods and observing deviations over time.
5. Document Calibration
- Record:
- The reference instrument details (serial number, last calibration date).
- The observed deviations and corrections made.
- Environmental conditions during calibration.
- The date and technician's name.
6. Schedule Routine Calibration
- Regularly calibrate the chamber (e.g., annually or as specified by quality standards).
By maintaining proper calibration, your humidity chamber will provide reliable and precise conditions for testing or storage.